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Methyl 4-chlorophenylacetate → 5-(4-Chloro-benzyl)-3-(1-methyl-4-phenyl-butyl)-3,6-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-7-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 4-chlorophenylacetate | HCID 104196 | — |
| 反応物 | 5-Amino-1-(1-methyl-4-phenyl-butyl)-1H-[1,2,3]triazole-4-carboxamide | HCID 11149992 | — |
| 生成物 | 5-(4-Chloro-benzyl)-3-(1-methyl-4-phenyl-butyl)-3,6-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-7-one | HCID 135528860 | — |
反応手順
Analogously to the procedure of Example 5, the title compound is prepared from 1.0 g (3.8 mmol) of 5-amino-1-(1-methyl-4-phenyl-butyl)-1H-[1,2,3]triazole-4-carboxamide and 1.83 g (10.7 mmol) of methyl 4-chlorophenylacetate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06458796B1 |
| 出典データセット | uspto-grants-2002_10 |
| ORD ID | ord-39bb2fd8f54246bba4901c7b1fb782c8 |
| 出典メモ | uspto-grants-2002_10 |