関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 1-Indanone | HCID 6735 | — |
| 反応物 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | Indan-1-one hydrazone | HCID 290932 | — |
反応手順
A mixture of indan-1-one (10.0 g), ethanol (35 ml), hydrazine hydrate (10.0 ml) and glacial acetic acid (2.0 ml) was boiled under reflux under nitrogen for 1 hour. The mixture was cooled to 20° C. and the mixture concentrated under reduced pressure to give a solid which was collected by filtration to give indan-1-one hydrazone, m.p. 84-86° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06462036B1 |
|---|
| 出典データセット | uspto-grants-2002_10 |
|---|
| ORD ID | ord-8fcf8b2ebf2e42ceae4bc6f390884184 |
|---|
| 出典メモ | uspto-grants-2002_10 |
|---|
