Acetic Acid → HCID 53812005、化合物
反応式
[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([NH:11][C:12](=[O:14])[CH3:13])=[CH:8][CH:9]=2)[CH2:4][CH2:3]1.[CH:15](=O)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1.C(O)(=O)C.N1CCCCC1>CO>[CH:15](=[C:3]1[CH2:4][C:5]2[C:10](=[CH:9][CH:8]=[C:7]([NH:11][C:12](=[O:14])[CH3:13])[CH:6]=2)[C:2]1=[O:1])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1参加物
6
実験手順
A mixture of N-(1-oxoindan-5-yl)acetamide (10.0 g, obtained from the Maybridge Chemical Co. Ltd), benzaldehyde (6.73 g), glacial acetic acid (1.06 g) and piperidine (10.8 g) was heated to 90° C. under nitrogen. Methanol (200 ml) was added and the mixture was cooled and then filtered to give N-(2-benzylidene-1-oxo-indan-5-yl)acetamide (13.47 g).
後処理
- customobtained from the Maybridge Chemical Co
- temperaturethe mixture was cooled
- filtrationfiltered
出典と根拠
- ORDレコード
- ord-a7e9ee60c9f1473f8addba167aa7d804
- 出典データセット
- uspto-grants-2002_10
- 特許番号
- US06462036B1
反応ノート
読み込み中…