化工社化工社 化学情報印刷レポート · 研究参考用
4-Methoxybenzenethiol → 2-(4-Methoxy-phenylsulfanyl)-tetradecanoic acid ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxybenzenethiol | HCID 12765 | — |
| 反応物 | Tetradecanoic acid, 2-bromo-, ethyl ester | HCID 85791 | — |
| 生成物 | 2-(4-Methoxy-phenylsulfanyl)-tetradecanoic acid ethyl ester | HCID 53881416 | 98% |
反応手順
2-(4-Methoxy-phenylsulfanyl)-tetradecanoic acid ethyl ester was prepared according to the general method as outlined in Example 1. Starting from the corresponding ethyl-2-bromomyristate (5.0 g, 14.9 mmol) and 4-methoxythiophenol (1.9 g, 13.4 mmol), 5.0 g of the product was isolated. Yield 98%; Light yellow oil; MS: 393 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06462073B2 |
| 出典データセット | uspto-grants-2002_10 |
| ORD ID | ord-6a0b56e948094d91bc76561a5509cc12 |
| 出典メモ | uspto-grants-2002_10 |