Hydroxide → 4,6-Dichloro-N-(1,1,3,3-tetramethylbutyl)-1,3,5-triazin-2-amine

HRID 992673

反応式

HRID 992673 の反応式
O.[N:2]1[C:9]([Cl:10])=[N:8][C:6](Cl)=[N:5][C:3]=1[Cl:4].[CH3:11][C:12]([NH2:19])([CH3:18])[CH2:13][C:14]([CH3:17])([CH3:16])[CH3:15].[OH-]>C1(C)C(C)=CC=CC=1>[Cl:10][C:9]1[N:2]=[C:3]([Cl:4])[N:5]=[C:6]([NH:19][C:12]([CH3:18])([CH3:11])[CH2:13][C:14]([CH3:17])([CH3:16])[CH3:15])[N:8]=1

参加物

6

反応物 4

HCID 961HydroxideHCID 962WaterHCID 7954Cyanuric chlorideHCID 61017tert-Octylamine

生成物 1

HCID 64308094,6-Dichloro-N-(1,1,3,3-tetramethylbutyl)-1,3,5-triazin-2-amine

試薬・触媒・溶媒 1

HCID 7237O-Xylene溶媒

実験手順

Into a flask, 20 grams of water, 50.0 grams (0.271 mole) of cyanuric chloride and 125 grams of a mixed xylene were charged and 35.9 grams (0.278 mole) of 1,1,3,3-tetramethylbutylamine was slowly and dropwise added into the mixture while keeping the temperature at 8-10° C. Then, 55.5 grams of a 20% aqueous hydroxide solution was slowly and dropwise added into the mixture while keeping the temperature at 8-10C. After the reaction was complete, the oil (organic) and water phases were separated and the water phase was separated off to obtain a xylene solution of 2,4-dichloro-6-(1,1,3,3-tetramethylbutylamino)-1,3,5-triazine.

後処理

  1. additiondropwise added into the mixture
  2. customat 8-10° C
  3. additiondropwise added into the mixture
  4. customthe oil (organic) and water phases were separated
  5. customthe water phase was separated off

出典と根拠

ORDレコード
ord-a255591dbbeb4858824a4f188aa8107d
出典データセット
uspto-grants-2002_10
特許番号
US06469165B1

関連ノート

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