2,4-Dimethyl-3-pentanone → HCID 18413318、化合物

反応式

[CH:1]([C:4]([CH:6]([CH3:8])[CH3:7])=[O:5])([CH3:3])[CH3:2].Cl[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH:15]1[CH2:20][CH:19]2[CH2:21][CH:16]1[CH:17]=[CH:18]2>>[CH:1]([C:4]([CH:6]([CH3:8])[CH3:7])([OH:5])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH:15]1[CH2:20][CH:19]2[CH2:21][CH:16]1[CH:17]=[CH:18]2)([CH3:3])[CH3:2]

参加物

反応物 2

HCID 112712,4-Dimethyl-3-pentanone

HCID 18410366HCID 18410366、化合物

生成物 1

HCID 18413318HCID 18413318、化合物収率 85%

実験手順

1,1-Diisopropyl-6-(5-norbornen-2-yl)hexanol (yield: 85%) was obtained in the same manner as in Synthesis Example 1, except that diisopropyl ketone and 1-chloro-5-(5-norbornen-2-yl)pentane were used in place of acetone and 1-chloro-4-(5-norbornen-2-yl)butane, respectively.

出典と根拠

ORDレコード: ord-061f0baec53f44608b9e014dcc5a504c
出典データセット: uspto-grants-2002_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06469220B2

反応ノート

読み込み中…