4-(tert-Butylaminosulphonyl)benzeneboronic acid → 4-(Aminosulphonyl)benzeneboronic acid
반응식
C([NH:5][S:6]([C:9]1[CH:14]=[CH:13][C:12]([B:15]([OH:17])[OH:16])=[CH:11][CH:10]=1)(=[O:8])=[O:7])(C)(C)C>C(O)(C(F)(F)F)=O.CCOCC>[NH2:5][S:6]([C:9]1[CH:10]=[CH:11][C:12]([B:15]([OH:17])[OH:16])=[CH:13][CH:14]=1)(=[O:8])=[O:7]참가 물질
4
실험 절차
A solution of 4-t-butylaminosulfonylbenzene boronic acid (500 mg) in TFA (5 mL) was stirred at r.t. for 15 h. The mixture was diluted with ether and the solid material was filtered to provide the title compound.
후처리
- filtrationthe solid material was filtered
출처 및 근거
- ORD 기록
- ord-07f470340be640ab8eb15f74be1c9dc0
- 출처 데이터셋
- uspto-grants-2000_04
- 특허 번호
- US06046217
반응 노트
불러오는 중…