Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methoxybenzaldehyde → alpha-(2-methoxyphenyl)-N-t-butylnitrone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methoxybenzaldehyde | HCID 8658 | — |
| 반응물 | N-tert-butylhydroxylamine | HCID 98586 | — |
| 생성물 | alpha-(2-methoxyphenyl)-N-t-butylnitrone | HCID 85447185 | — |
반응 단계
The title compound was prepared according to the procedure described in Example 7 using 2-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 82.9% overall yield as white crystals, m.p. 109.1 ° C. (Rf =0.53 on a silica gel plate using ethyl acetate as the eluant).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06046232 |
| 출처 데이터셋 | uspto-grants-2000_04 |
| ORD ID | ord-619ea8b4edd344849d580107504db57f |
| 출처 메모 | uspto-grants-2000_04 |