2-Methylimidazole → 2-Methyl-1-(4-nitrobenzyl)-1H-imidazole

HRID 1004150노트

반응식

[CH3:1][C:2]1[NH:3][CH:4]=[CH:5][N:6]=1.[N+:7]([C:10]1[CH:21]=[CH:20][C:13]([CH2:14]C2NC=CN=2)=[CH:12][CH:11]=1)([O-:9])=[O:8]>>[CH3:1][C:2]1[N:3]([CH2:14][C:13]2[CH:20]=[CH:21][C:10]([N+:7]([O-:9])=[O:8])=[CH:11][CH:12]=2)[CH:4]=[CH:5][N:6]=1

참가 물질

반응물 2

HCID 127492-Methylimidazole

HCID 104428612-(4-NITRO-BENZYL)-1H-IMIDAZOLE

생성물 1

HCID 50471292-Methyl-1-(4-nitrobenzyl)-1H-imidazole수율 61.7%

실험 절차

15.2 g of 2-methylimidazole and 40.7 g of 4-nitrobenzylimidazole were subjected to an alkylation reaction to obtain 24.8 g of 2-methyl-1-(4-nitrobenzyl)imidazole.

출처 및 근거

ORD 기록: ord-b0e73c9abc05426d94cf373a23379ce8
출처 데이터셋: uspto-grants-2000_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06048884

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