Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → Methyl (2-chlorophenyl)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | o-Chlorophenylacetic acid | HCID 17124 | — |
| 촉매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | Methyl (2-chlorophenyl)acetate | HCID 93683 | — |
반응 단계
A solution of 2-chlorophenylacetic acid (10.0 g) in methanol (100 ml) containing 1 drop of concentrated sulphuric acid was heated at reflux for 2 hours. The reaction mixture was evaporated to half volume and partitioned between ethyl acetate (100 ml) and water (100 ml). The organic phase was dried over magnesium sulphate and evaporated to give the title compound (10.0 g) as a colourless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06048893 |
| 출처 데이터셋 | uspto-grants-2000_04 |
| ORD ID | ord-9fca659e73f847a3a5eb5a0804ca6a53 |
| 출처 메모 | uspto-grants-2000_04 |