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Ammonium Chloride → HCID 178488155, 화합물

HRID 1004404
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HRID 1004404 반응식
[CH3:1][C:2]1[CH:3]=[N:4][C:5]([CH2:11][S+:12]([O-:24])[C:13]2[NH:14][C:15]3[CH:16]=[CH:17][C:18]([O:22][CH3:23])=[CH:19][C:20]=3[N:21]=2)=[C:6]([CH3:10])[C:7]=1[O:8][CH3:9].[Cl-].[Mg+2].[Cl-].[Cl-].[NH4+:29]>N>[CH3:1][C:2]1[CH:3]=[N:4][C:5]([CH2:11][S+:12]([O-:24])[C:13]2[NH:14][C:15]3[CH:16]=[CH:17][C:18]([O:22][CH3:23])=[CH:19][C:20]=3[N:21]=2)=[C:6]([CH3:10])[C:7]=1[O:8][CH3:9].[NH3:29]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 25517Ammonium ChlorideHCID 5360315Magnesium ChlorideHCID 178488147HCID 178488147, 화합물2회

생성물 1

HCID 178488155HCID 178488155, 화합물

시약·촉매·용매 1

HCID 222Ammonia용매2회

실험 절차

In the process of the invention, it is preferred to pre-form a solution of omeprazole in concentrated ammonia, and to add this to a pre-formed aqueous solution of magnesium salt (preferably magnesium chloride) and ammonium salt (preferably ammonium chloride), so that the magnesium ion is in excess during the mixing procedure. However, other orders of addition can be used if the process is conducted carefully, such as mixing the omeprazole, ammonia and ammonium salt first, and adding the magnesium salt to this mixture, or, less desirably, pre-mixing the magnesium salt and ammonium salt, and adding this mixture to pre-formed omeprazole/ammonia solution.

후처리

  1. additionHowever, other orders of addition
  2. additionadding this mixture

출처 및 근거

ORD 기록
ord-138450476fed447f9ca63b57449a9eca
출처 데이터셋
uspto-grants-2000_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06048981

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