3-[(5-Carboxy-furan-2-ylmethyl)-amino]-phthalic acid dimethyl ester → 3-[(5-Carboxy-furan-2-ylmethyl)-amino]-phthalic acid

HRID 10046

반응식

HRID 10046 반응식
C[O:2][C:3](=[O:24])[C:4]1[C:5](=[C:10]([NH:14][CH2:15][C:16]2[O:17][C:18]([C:21]([OH:23])=[O:22])=[CH:19][CH:20]=2)[CH:11]=[CH:12][CH:13]=1)[C:6]([O:8]C)=[O:7].COCCNC1C=CC=C(C(O)=O)C=1C(O)=O>>[C:21]([C:18]1[O:17][C:16]([CH2:15][NH:14][C:10]2[CH:11]=[CH:12][CH:13]=[C:4]([C:3]([OH:24])=[O:2])[C:5]=2[C:6]([OH:8])=[O:7])=[CH:20][CH:19]=1)([OH:23])=[O:22]

참가 물질

3

반응물 2

HCID 210401283-[(5-Carboxy-furan-2-ylmethyl)-amino]-phthalic acid dimethyl esterHCID 219885193-(2-Methoxy-ethylamino)-phthalic acid

생성물 1

HCID 219886173-[(5-Carboxy-furan-2-ylmethyl)-amino]-phthalic acid

실험 절차

3-[(5-Carboxy-furan-2-ylmethyl)-amino]-phthalic acid dimethyl ester (0.90 g, 2.70 mmol) was treated in the same manner as described above for the synthesis of 3-(2-methoxy-ethylamino)-phthalic acid. The product of the reaction, which contained a mixture of diacid and monomethyl esters, was used without further purification.

후처리

  1. customThe product of the reaction, which
  2. customwas used without further purification

출처 및 근거

ORD 기록
ord-a080fa42b94c4d4aa5467f846ef27407
출처 데이터셋
uspto-grants-2006_08
특허 번호
US07091353B2

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