Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → Ethyl 2-(9-xanthyl)-3-oxo-3-[3-(phenacylmethyloxycarbonyl)cyclobutyl]propanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Xanthydrol | HCID 72861 | — |
| 반응물 | Ethyl 3-oxo-3-[3-(phenacylmethyloxycarbonyl) cyclobutyl]propanate | HCID 18791135 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Ethyl 2-(9-xanthyl)-3-oxo-3-[3-(phenacylmethyloxycarbonyl)cyclobutyl]propanate | HCID 18791133 | — |
반응 단계
Acetic acid (20 ml) was added to a stirred suspension of 9-hydroxyxanthene (3.96 g, 20 mmol) and ethyl 3-oxo-3-[3-(phenacylmethyloxycarbonyl) cyclobutyl]propanate (6.0 g, 18 mmol) in ethanol (20 ml) at room temperature. A clear solution formed and was allowed to stand for 7 days at room temperature.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06054448 |
| 출처 데이터셋 | uspto-grants-2000_04 |
| ORD ID | ord-d2a13ead311f457bbe212e4d69a20f70 |
| 출처 메모 | uspto-grants-2000_04 |