Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methoxycyclohexene → 5-(3,5-Dimethylphenylthio)-4-isopropyl-1-[2-(1-methoxycyclohexyloxy)ethoxymethyl)-2-methyl-1H-imidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methoxycyclohexene | HCID 70264 | — |
| 반응물 | 2-[5-(3,5-Dimethyl-phenylsulfanyl)-4-isopropyl-2-methyl-imidazol-1-ylmethoxy]-ethanol | HCID 478180 | — |
| 생성물 | 5-(3,5-Dimethylphenylthio)-4-isopropyl-1-[2-(1-methoxycyclohexyloxy)ethoxymethyl)-2-methyl-1H-imidazole | HCID 15887185 | 74.9% |
반응 단계
The compound 1 (502 mg, 1.50 mmol) was converted to the acetal with 1-methoxycyclohexene (1.68 g, 15.0 mmol) in the same manner as the example 2 to give the compound 3 (502 mg, 72%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06054591 |
| 출처 데이터셋 | uspto-grants-2000_04 |
| ORD ID | ord-041186c113bc459a9d99051af14fa557 |
| 출처 메모 | uspto-grants-2000_04 |