Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1-Dibutoxycyclohexane → 2-[(1-Butoxycyclohexyloxy)methyl]-5-(3,5-dichlorophenylthio)-4-isopropyl-1-methyl-1H-imidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1-Dibutoxycyclohexane | HCID 243718 | — |
| 반응물 | (5-(3,5-Dichlorophenylthio)-4-isopropyl-1-methyl-1H-imidazol-2-yl)methanol | HCID 473916 | — |
| 생성물 | 2-[(1-Butoxycyclohexyloxy)methyl]-5-(3,5-dichlorophenylthio)-4-isopropyl-1-methyl-1H-imidazole | HCID 18792012 | 30.9% |
반응 단계
The compound 14 (3.1 mg, 0.1 mmol) was converted to the acetal with 1,1-dibutoxycyclohexane (228 mg, 1 mmol) in the same manner as the example 14 to give the compound 16 (15 mg, 30%) as oil. Rf 0.44 (Al2O3 60, Type E, toluene).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06054591 |
| 출처 데이터셋 | uspto-grants-2000_04 |
| ORD ID | ord-b2ab2a707f264b7a858f4e433d52e597 |
| 출처 메모 | uspto-grants-2000_04 |