Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1-Dibutoxycyclohexane → 2-(1-Butoxycyclohexyloxy)methyl-5-(3,5-dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1-Dibutoxycyclohexane | HCID 243718 | — |
| 반응물 | (5-(3,5-Dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazol-2-yl)methanol | HCID 473933 | — |
| 생성물 | 2-(1-Butoxycyclohexyloxy)methyl-5-(3,5-dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazole | HCID 18792052 | 35% |
반응 단계
The compound 19 (345 mg, 1.00 mmol) was converted to the acetal with 1,1-dibutoxycyclohexane (2.28 g, 10.0 mmol) in the same manner as the example 18 to give the compound 21 (172 mg, 35%) as oil. Rf 0.41 (Al2O3 60, Type E, toluene).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06054591 |
| 출처 데이터셋 | uspto-grants-2000_04 |
| ORD ID | ord-b97b14f4d45547458ad5b9ca3ec6d6e1 |
| 출처 메모 | uspto-grants-2000_04 |