Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methoxycyclohex-2-en-1-one → 3-Butylcyclohex-2-en-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methoxycyclohex-2-en-1-one | HCID 85597 | — |
| 반응물 | Butyllithium | HCID 178418339 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 3-Butylcyclohex-2-en-1-one | HCID 239095 | 97.2% |
반응 단계
The general procedure for the preparation of substrates using 3-methoxycyclohexenone (1.26 g, 10 mmol) and n-BuLi (20 mmol, 1.6 M in hexane) gave, after flash chromatography (4:1 hexanes:ethyl acetate) the title compound as a colorless liquid (1.48 g, 97%). Spectroscopic data were consistent with previously reported data for this compound.2
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06787655B2 |
| 출처 데이터셋 | uspto-grants-2004_09 |
| ORD ID | ord-79012498f96c4523b95f6a25de9f0d83 |
| 출처 메모 | uspto-grants-2004_09 |