Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Urea → 1,3(2H,4H)-isoquinolinedione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Urea | HCID 1176 | — |
| 반응물 | Homophthalic anhydride | HCID 12801 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1,3(2H,4H)-isoquinolinedione | HCID 349435 | 52.8% |
반응 단계
Homophthalic anhydride (20 g) and urea (60 g) were reacted at 170° C. for 1 hr. The reaction mixture was cooled, water (500 ml) was added thereto, and then the resulting precipitates were collected by filtration. The precipitate were washed with water and dried in hot air, to give 10.5 g of homophthalimide as a white powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06790844B2 |
| 출처 데이터셋 | uspto-grants-2004_09 |
| ORD ID | ord-eed351f54faa42abad5759f85dee4ab7 |
| 출처 메모 | uspto-grants-2004_09 |