Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → HCID 86588302, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | Sulfamethoxazole | HCID 5329 | — |
| 용매 | Methanol | HCID 887 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 86588302 | HCID 86588302 | 60% |
반응 단계
The compound is prepared by starting from a Sulfamethoxazole solution (2 g, 7.9 mmoli) in methanol (100 ml), addition of a 65% nitric acid solution (0.500 ml) in acetonitrile (5 ml), following the procedure reported in Example 5. Sulfamethoxazole nitrate as amorphous solid is obtained. Yield 60%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06794372B2 |
| 출처 데이터셋 | uspto-grants-2004_09 |
| ORD ID | ord-7e868392ac6d4e0dbe7cd7f6fb4e6bd2 |
| 출처 메모 | uspto-grants-2004_09 |