4-Methyl-2-nitroaniline → 6-Chloro-N-(4-methyl-2-nitrophenyl)-3-pyridinecarboxamide

HRID 1007185

반응식

HRID 1007185 반응식
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][N:3]=1.[CH3:11][C:12]1[CH:18]=[CH:17][C:15]([NH2:16])=[C:14]([N+:19]([O-:21])=[O:20])[CH:13]=1>>[Cl:1][C:2]1[N:3]=[CH:4][C:5]([C:6]([NH:16][C:15]2[CH:17]=[CH:18][C:12]([CH3:11])=[CH:13][C:14]=2[N+:19]([O-:21])=[O:20])=[O:7])=[CH:9][CH:10]=1

참가 물질

3

반응물 2

HCID 69784-Methyl-2-nitroanilineHCID 27821656-Chloronicotinoyl Chloride

생성물 1

HCID 98145676-Chloro-N-(4-methyl-2-nitrophenyl)-3-pyridinecarboxamide

실험 절차

The title compound was prepared from 6-chloronicotinoyl chloride and 4-methyl-2-nitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (CDCl3): 11.29 (s, 1H), 9.02 (d, J=2.7, 1H), 8.81 (d, J=8.7, 1H), 8.24-8.21 (m, 1H), 8.11 (s, 1H), 7.58-7.50 (m, 2H), 2.44 (s, 3H).

후처리

  1. customwas obtained as a yellow solid

출처 및 근거

ORD 기록
ord-bfb15b91f700496dbd58eeb4bf19c1c4
출처 데이터셋
uspto-grants-2004_09
특허 번호
US06794397B2

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