Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(6-Amino-1,3-benzodioxol-5-yl)ethan-1-one → N-(6-acetylbenzo[d][1,3]dioxol-5-yl)-6-chloronicotinamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(6-Amino-1,3-benzodioxol-5-yl)ethan-1-one | HCID 120000 | — |
| 반응물 | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| 생성물 | N-(6-acetylbenzo[d][1,3]dioxol-5-yl)-6-chloronicotinamide | HCID 22668937 | — |
반응 단계
The title compound was prepared from 6-chloronicotinoyl chloride and 2-amino-4,5-methylenedioxyacetophenone as a light grey-yellow solid as described in Example 1. 1H NMR (CDCl3): 9.09-9.08 (m, 1H), 8.55 (s, 1H), 8.30-8.27 (m, 1H), 7.50-7.47 (m, 1H), 7.35 (s, 1H), 6.10 (s, 2H), 2.64 (s, 3H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06794397B2 |
| 출처 데이터셋 | uspto-grants-2004_09 |
| ORD ID | ord-da1a5f409be0466eb2ef2b96eccfe875 |
| 출처 메모 | uspto-grants-2004_09 |