Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-2-methyl-6-nitroaniline → HCID 22668925, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-2-methyl-6-nitroaniline | HCID 182355 | — |
| 반응물 | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| 생성물 | HCID 22668925 | HCID 22668925 | — |
반응 단계
The title compound was prepared from 4-chloro-2-methyl-6-nitroaniline (204 mg, 1.09 mmol) and 6-chloronicotinoyl chloride (192 mg, 1.09 mmol) and obtained as a light yellow solid as described in Example 62. 1H NMR (CDCl3): 9.13 (s, 1H), 8.96 (dd, J=0.6, 2.4 Hz, 1H), 8.20 (dd, J=2.7, 8.4 Hz, 1H), 7.93 (d, J=2.4 Hz, 1H), 7.59 (d, J=2.4 Hz, 1H), 7.51 (dd, J=0.6, 8.1 Hz, 1H), 2.38 (s, 3H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06794397B2 |
| 출처 데이터셋 | uspto-grants-2004_09 |
| ORD ID | ord-ec54ddd7cc5543d6b06139b5a426c519 |
| 출처 메모 | uspto-grants-2004_09 |