3-Furoic acid → N-(4-Ethoxy-2-nitrophenyl)-3-furancarboxamide

HRID 1007232노트

반응식

HRID 1007232 반응식
[O:1]1[CH:5]=[CH:4][C:3]([C:6]([OH:8])=O)=[CH:2]1.[CH2:9]([O:11][C:12]1[CH:18]=[CH:17][C:15]([NH2:16])=[C:14]([N+:19]([O-:21])=[O:20])[CH:13]=1)[CH3:10]>>[CH2:9]([O:11][C:12]1[CH:18]=[CH:17][C:15]([NH:16][C:6]([C:3]2[CH:4]=[CH:5][O:1][CH:2]=2)=[O:8])=[C:14]([N+:19]([O-:21])=[O:20])[CH:13]=1)[CH3:10]

참가 물질

3

반응물 2

HCID 102683-Furoic acidHCID 692294-Ethoxy-2-nitroaniline

생성물 1

HCID 9943482N-(4-Ethoxy-2-nitrophenyl)-3-furancarboxamide

실험 절차

The title compound was prepared from 3-furoic acid and 4-ethoxy-2-nitroaniline as a yellow solid as described in Example 15. 1H NMR (DMSO-d6): 10.25 (s, 1H), 8.36 (d, J=2.4, 1H), 7.83-7.81 (m, 1H), 7.53-7.47 (m, 2H), 7.35-7.31 (m, 1H), 6.94 (d, J=2.4, 1H), 4.12 (q, J=6.9, 2H), 1.35 (t, J=6.9, 3H).

출처 및 근거

ORD 기록
ord-7ea257e44ccf41158ff9d536679e2aac
출처 데이터셋
uspto-grants-2004_09
특허 번호
US06794397B2

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