Urocanic Acid → HCID 178525356, 화합물

HRID 1008667노트

반응식

HRID 1008667 반응식
[CH:1]1[N:5]=[CH:4][NH:3][C:2]=1/[CH:6]=[CH:7]/[C:8]([OH:10])=[O:9]>[Pd].CO>[NH:5]1[CH:1]=[C:2]([CH2:6][CH2:7][C:8]([OH:10])=[O:9])[N:3]=[CH:4]1

참가 물질

4

반응물 1

HCID 736715Urocanic Acid2회

생성물 1

HCID 178525356HCID 178525356, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

Urocanic acid (3-(1H-imidazol-4-yl)-acrylic acid) (138 mg, 1 mmol) was placed in a round-bottom flask and dist MeOH was added thereto until urocanic acid was completely dissolved. To this solution, 10% Pd/C (30 mg) was added, replaced with H2 and stirred. After five hours, the loss of raw materials was confirmed, filtered, and the filtrate was concentrated under a reduced pressure to give the objective product.

후처리

  1. filtrationfiltered
  2. concentrationthe filtrate was concentrated under a reduced pressure
  3. customto give the objective product

출처 및 근거

ORD 기록
ord-007396ff74da472dba05514217e4cb3d
출처 데이터셋
uspto-grants-2011_07
특허 번호
US07973027B2

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