Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Azobisisobutyronitrile → Butyl Acrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | Butyl Acrylate | HCID 8846 | — |
| 반응물 | 2-Hydroxyethyl acrylate | HCID 13165 | — |
| 반응물 | Stearyl acrylate | HCID 62552 | — |
| 용매 | Toluene | HCID 1140 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | Butyl Acrylate | HCID 8846 | — |
| 생성물 | Stearyl acrylate | HCID 62552 | — |
| 생성물 | HCID 178473601 | HCID 178473601 | — |
반응 단계
To a 1 L flask equipped with a stirrer, a nitrogen introducing tube, a thermometer and a condenser, 50 g of stearyl acrylate, 49 g of n-butylacrylate, 1 g of hydroxyethyl acrylate, 0.89 g of AIBN, 100 mL of toluene and 100 mL of ethyl acetate were added and subjected to polymerization reaction in a stream of nitrogen at 70° C. for 12 hr, to obtain a copolymer of stearyl acrylate, n-butyl acrylate and hydroxyacrylate (hereinafter sometimes referred to “PSABAHEA”. The resulting PSABAHEA had a weight average molecular weight of 170,000.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07976921B2 |
| 출처 데이터셋 | uspto-grants-2011_07 |
| ORD ID | ord-8bc452f0ce8242eeb56d756833558e2b |
| 출처 메모 | uspto-grants-2011_07 |