Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Anisoyl chloride → 2-Fluoro-4'-methoxybenzophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Anisoyl chloride | HCID 7477 | — |
| 반응물 | Anisole | HCID 7519 | — |
| 반응물 | 1-Naphthylamine | HCID 8640 | — |
| 반응물 | 2-Fluorobenzoyl chloride | HCID 9808 | — |
| 생성물 | 2-Fluoro-4'-methoxybenzophenone | HCID 2783236 | — |
반응 단계
The procedure of Example 10 was followed except as follows. In Part A, 1-amino napthalene (47 g) was used in place of 4-methoxy aniline. In Step 1 of Part B, 2-fluorobenzoyl chloride (15.8 g) and anisole (10.8 g) were used in place of 1,3-dimethoxybenezene and p-anisoyl chloride respectively to produce (2-fluoro-phenyl)-(4-methoxy-phenyl)-methanone. An NMR spectrum showed the final product to have a structure consistent with 12-ethoxy-3-(2-fluorophenyl)-3-(4-methoxy)-3H-benzo[h]pyrano[3,2-c]quinoline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07094368B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-2b20b70246a44d1e8b70b50336b7441c |
| 출처 메모 | uspto-grants-2006_08 |