Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(Diethylamino)pyrrolidine → [5-(3-bromo-phenyl)-1,4-dimethyl-1H-pyrazol-3-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(Diethylamino)pyrrolidine | HCID 19961995 | — |
| 반응물 | 5-(3-bromo-phenyl)-1,4-dimethyl-1H-pyrazole-3-carboxylic acid | HCID 67315328 | — |
| 생성물 | [5-(3-bromo-phenyl)-1,4-dimethyl-1H-pyrazol-3-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone | HCID 67315151 | 94% |
반응 단계
In analogy to the procedure described in example 12D], 5-(3-bromo-phenyl)-1,4-dimethyl-1H-pyrazole-3-carboxylic acid and 3-(diethylamino)pyrrolidine gave the title compound in 94% yield as white needles. MS: 419.2 (MH+, 1 Br).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07977358B2 |
| 출처 데이터셋 | uspto-grants-2011_07 |
| ORD ID | ord-289c11f5102c4cb2ae58ef35805e8b61 |
| 출처 메모 | uspto-grants-2011_07 |