Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(3-Bromophenyl)-3,5-dimethyl-1H-pyrazole-4-carboxylic acid → [1-(3-Bromo-phenyl)-3,5-dimethyl-1H-pyrazol-4-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(3-Bromophenyl)-3,5-dimethyl-1H-pyrazole-4-carboxylic acid | HCID 2763997 | — |
| 반응물 | 3-(Diethylamino)pyrrolidine | HCID 19961995 | — |
| 생성물 | [1-(3-Bromo-phenyl)-3,5-dimethyl-1H-pyrazol-4-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone | HCID 67313795 | 61% |
반응 단계
In analogy to the procedure described in example 12D], 1-(3-bromo-phenyl)-3,5-dimethyl-1H-pyrazole-4-carboxylic acid and 3-(diethylamino)pyrrolidine gave the title compound in 61% yield as brown viscous oil. MS: 419.2 (MH+, 1 Br).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07977358B2 |
| 출처 데이터셋 | uspto-grants-2011_07 |
| ORD ID | ord-c4300c4424d042559fff4078a37aabac |
| 출처 메모 | uspto-grants-2011_07 |