Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
trans-2-(4-Chlorophenyl)vinylboronic acid → HCID 57554998, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | trans-2-(4-Chlorophenyl)vinylboronic acid | HCID 642694 | — |
| 반응물 | [1-(3-Bromo-phenyl)-3,5-dimethyl-1H-pyrazol-4-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone | HCID 67313795 | — |
| 생성물 | HCID 57554998 | HCID 57554998 | 67% |
반응 단계
In analogy to the procedure described in Example 14C], [1-(3-bromo-phenyl)-3,5-dimethyl-1H-pyrazol-4-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone (Example 28A]) and trans-2-(4-chlorophenyl)vinylboronic acid gave the title compound in 67% yield as light brown foam. MS: 477.3 (MH+, 1 Cl).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07977358B2 |
| 출처 데이터셋 | uspto-grants-2011_07 |
| ORD ID | ord-04b8153fdbc94b5e99b877891c9a8e96 |
| 출처 메모 | uspto-grants-2011_07 |