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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 10122생성일: 2026년 10월 23일

4'-Methoxyacetophenone → 1-(4-Methoxy-phenyl)-5-phenyl-penta-2,4-diene-1-one

https://huagongshe.com/ko/reaction/10122

반응식

참여 물질

역할이름HCID투입량
반응물4'-MethoxyacetophenoneHCID 7476—
반응물Sodium HydroxideHCID 14798—
반응물CinnamaldehydeHCID 637511—
용매EthanolHCID 702—
생성물1-(4-Methoxy-phenyl)-5-phenyl-penta-2,4-diene-1-oneHCID 339666072%

반응 단계

2 ml of trans-cinnamaldehyde and 2.5 g of 4-methoxy acetophenone were dissolved in 50 ml of ethanol at room temperature. 10 ml of sodium hydroxide solution was then added and stirred for 12 h to form yellow solid precipitation. Filtering the precipitation to obtain the compound 1, with yield of 72% and purity of 96.3%. FIG. 1 and FIG. 2 respectively show the NMR and UV spectrum of compound 1; wherein the maximum adsorptive wavelength of compound 1 is 345 nm, and the adsorptive coefficient ε is 4.5×104, both listed on Table 1.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07094457B2
출처 데이터셋uspto-grants-2006_08
ORD IDord-8515cfed68d2474e998cef70299e4581
출처 메모uspto-grants-2006_08