Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4'-Methoxyacetophenone → 1-(4-Methoxy-phenyl)-5-phenyl-penta-2,4-diene-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4'-Methoxyacetophenone | HCID 7476 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Cinnamaldehyde | HCID 637511 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-(4-Methoxy-phenyl)-5-phenyl-penta-2,4-diene-1-one | HCID 3396660 | 72% |
반응 단계
2 ml of trans-cinnamaldehyde and 2.5 g of 4-methoxy acetophenone were dissolved in 50 ml of ethanol at room temperature. 10 ml of sodium hydroxide solution was then added and stirred for 12 h to form yellow solid precipitation. Filtering the precipitation to obtain the compound 1, with yield of 72% and purity of 96.3%. FIG. 1 and FIG. 2 respectively show the NMR and UV spectrum of compound 1; wherein the maximum adsorptive wavelength of compound 1 is 345 nm, and the adsorptive coefficient ε is 4.5×104, both listed on Table 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07094457B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-8515cfed68d2474e998cef70299e4581 |
| 출처 메모 | uspto-grants-2006_08 |