Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Carbonate → 5-(2-bromophenyl)-1H-pyrrole-3-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | (2-Bromophenyl)boronic acid | HCID 2773294 | — |
| 반응물 | 5-bromo-1H-pyrrole-3-carbaldehyde | HCID 57831983 | — |
| 촉매 | HCID 178418397 | HCID 178418397 | — |
| 생성물 | 5-(2-bromophenyl)-1H-pyrrole-3-carbaldehyde | HCID 86630989 | — |
반응 단계
By a similar operation as in Reference Example 148 and using 5-bromo-1H-pyrrole-3-carbaldehyde (870 mg), (2-bromophenyl)boronic acid (1.20 g), sodium carbonate (1.27 g) and tetrakis(triphenylphosphine)palladium (289 mg), the title compound was obtained as colorless crystals (yield 396 mg, 32%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07977488B2 |
| 출처 데이터셋 | uspto-grants-2011_07 |
| ORD ID | ord-0a214f4e4b7e4d9ea8ee78b75bd8e3ec |
| 출처 메모 | uspto-grants-2011_07 |