Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Styrene Oxide → 2-(2-(3-(2-Hydroxy-2-phenylethoxy)phenoxy)ethyl)isoindoline-1,3-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Styrene Oxide | HCID 7276 | — |
| 반응물 | 2-[2-(3-Hydroxy-phenoxy)-ethyl]-isoindole-1,3-dione | HCID 58027534 | — |
| 생성물 | 2-(2-(3-(2-Hydroxy-2-phenylethoxy)phenoxy)ethyl)isoindoline-1,3-dione | HCID 67317562 | — |
반응 단계
Alkylation reaction of phenol 24 with styrene oxide gave 2-(2-(3-(2-hydroxy-2-phenylethoxy)phenoxy)ethyl)isoindoline-1,3-dione as yellow oil. Yield (0.85 g, 50%): 1H NMR (400 MHz, CDCl3) δ 7.99 (d, J=7.2 Hz, 1H), 7.41-7.53 (m, 3H), 7.28-7.38 (m, 5H), 7.12-7.16 (m, 1H), 6.60-6.65 (m, 1H), 6.52 (s, 1H), 6.48 (dd, J=8.0, 2.0 Hz, 1H), 4.79-4.82 (m, 1H), 4.19 (t, J=5.4 Hz, 2H), 3.72-3:84 (m, 4H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07982071B2 |
| 출처 데이터셋 | uspto-grants-2011_07 |
| ORD ID | ord-ffb3399c02b04797984f2d609170a69b |
| 출처 메모 | uspto-grants-2011_07 |