Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(1-Methyl-1H-imidazol-4-yl)ethanamine bis(4-methylbenzenesulfonate) → 1-Methylhistamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(1-Methyl-1H-imidazol-4-yl)ethanamine bis(4-methylbenzenesulfonate) | HCID 86254824 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1-Methylhistamine | HCID 3614 | — |
반응 단계
[2-(1-methyl-1H-imidazol-4-yl)ethyl]amine bis(4-methylbenzenesulfonate) (50 g) was dissolved in IMS (200 ml)/water (200 ml). This was passed through a DOWEX550A column (600 g), eluting with IMS (ca. 4 litres). Appropriate fractions were combined and concentrated in vacuo to yield the title compound, 13.4 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07985740B2 |
| 출처 데이터셋 | uspto-grants-2011_07 |
| ORD ID | ord-f3da4045887c466dbdc32a66a7e10fda |
| 출처 메모 | uspto-grants-2011_07 |