Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-3-methoxy-2-methylpyridine → 4-(3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-yloxy)-3-methoxy-2-methylpyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-3-methoxy-2-methylpyridine | HCID 10583046 | — |
| 반응물 | 3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-ol | HCID 12470096 | — |
| 생성물 | 4-(3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-yloxy)-3-methoxy-2-methylpyridine | HCID 19693934 | 75% |
반응 단계
Preparation was carried out analogously to Example 43 from 4-chloro-3-methoxy-2-methylpyridine and 3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-ol. Yield: 75%; M.p.: 90° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05723450 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-23dc3d980fa24e5c82e553d717c3da9c |
| 출처 메모 | uspto-grants-1998_03 |