4-Chloro-3-methoxy-2-methylpyridine → 4-(3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-yloxy)-3-methoxy-2-methylpyridine

HRID 1015

반응식

HRID 1015 반응식
Cl[C:2]1[CH:7]=[CH:6][N:5]=[C:4]([CH3:8])[C:3]=1[O:9][CH3:10].[CH3:11][C:12]1([CH3:24])[CH2:17][O:16][C:15]2([CH2:22][CH2:21][CH:20]([OH:23])[CH2:19][CH2:18]2)[O:14][CH2:13]1>>[CH3:11][C:12]1([CH3:24])[CH2:13][O:14][C:15]2([CH2:18][CH2:19][CH:20]([O:23][C:2]3[CH:7]=[CH:6][N:5]=[C:4]([CH3:8])[C:3]=3[O:9][CH3:10])[CH2:21][CH2:22]2)[O:16][CH2:17]1

참가 물질

3

반응물 2

HCID 105830464-Chloro-3-methoxy-2-methylpyridineHCID 124700963,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-ol

생성물 1

HCID 196939344-(3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-yloxy)-3-methoxy-2-methylpyridine수율 75%

실험 절차

Preparation was carried out analogously to Example 43 from 4-chloro-3-methoxy-2-methylpyridine and 3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-ol. Yield: 75%; M.p.: 90° C.

후처리

  1. customPreparation

출처 및 근거

ORD 기록
ord-23dc3d980fa24e5c82e553d717c3da9c
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05723450

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