Aluminium lithium hydride → 1,3-Benzodioxole-4-ethanamine

HRID 1015006노트

반응식

HRID 1015006 반응식
[N+:1]([CH:4]=[CH:5][C:6]1[C:14]2[O:13][CH2:12][O:11][C:10]=2[CH:9]=[CH:8][CH:7]=1)([O-])=O.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[O:11]1[C:10]2[CH:9]=[CH:8][CH:7]=[C:6]([CH2:5][CH2:4][NH2:1])[C:14]=2[O:13][CH2:12]1

참가 물질

3

반응물 2

HCID 21226445Aluminium lithium hydrideHCID 545432424-(2-Nitroethenyl)-2H-1,3-benzodioxole

생성물 1

HCID 152349621,3-Benzodioxole-4-ethanamine

실험 절차

In close analogy to the procedure described above, 4-(2-Nitro-vinyl)-benzo[1,3]dioxole is reacted with lithium aluminium hydride to provide the title compound.

출처 및 근거

ORD 기록
ord-6348872daaa54daa924f5f83fdc04e0b
출처 데이터셋
uspto-grants-2011_07
특허 번호
US07985753B2

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