Phosphorus oxide (P4O10) → 5-Methoxy-1-methyl-3,4-dihydroisoquinoline

HRID 1015040노트

반응식

HRID 1015040 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH2:9][CH2:10][NH:11][C:12](=O)[CH3:13].O=P12OP3(OP(OP(O3)(O1)=O)(=O)O2)=O>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]2[C:4]=1[CH2:9][CH2:10][N:11]=[C:12]2[CH3:13]

참가 물질

3

반응물 2

HCID 14812Phosphorus oxide (P4O10)HCID 4053755N-[2-(2-methoxyphenyl)ethyl]acetamide

생성물 1

HCID 450911955-Methoxy-1-methyl-3,4-dihydroisoquinoline

실험 절차

In close analogy to the procedure described above, N-[2-(2-methoxy-phenyl)-ethyl]-acetamide is reacted with phosphorus pentoxide to provide the title compound.

출처 및 근거

ORD 기록
ord-960451b4c21e46e08e30f2549d789984
출처 데이터셋
uspto-grants-2011_07
특허 번호
US07985753B2

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