Phosphorus oxide (P4O10) → 1-Methyl-5,6-dimethoxy-3,4-dihydro-isoquinoline
반응식
[CH3:1][O:2][C:3]1[C:8]([O:9][CH3:10])=[CH:7][CH:6]=[CH:5][C:4]=1[CH2:11][CH2:12][NH:13][C:14](=O)[CH3:15].O=P12OP3(OP(OP(O3)(O1)=O)(=O)O2)=O>>[CH3:1][O:2][C:3]1[C:8]([O:9][CH3:10])=[CH:7][CH:6]=[C:5]2[C:4]=1[CH2:11][CH2:12][N:13]=[C:14]2[CH3:15]참가 물질
3
실험 절차
In close analogy to the procedure described above, N-[2-(2,3-dimethoxy-phenyl)-ethyl]-acetamide is reacted with phosphorus pentoxide to provide the title compound.
출처 및 근거
- ORD 기록
- ord-cc04a783188940a299525ce224b3a216
- 출처 데이터셋
- uspto-grants-2011_07
- 특허 번호
- US07985753B2
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