Sodium triacetoxyborohydride → 1,7-Dimethyl-1,2,3,4-tetrahydroisoquinoline

HRID 1015049노트

반응식

[CH3:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[C:9]([CH3:12])[CH:10]=2)[CH2:5][CH2:4][N:3]=1.C(O[BH-](OC(=O)C)OC(=O)C)(=O)C.[Na+]>>[CH3:1][CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[C:9]([CH3:12])[CH:10]=2)[CH2:5][CH2:4][NH:3]1

참가 물질

반응물 2

HCID 5049666Sodium triacetoxyborohydride

HCID 59458304HCID 59458304, 화합물

생성물 1

HCID 242574291,7-Dimethyl-1,2,3,4-tetrahydroisoquinoline

실험 절차

In close analogy to the procedure described above, 1,7-dimethyl-3,4-dihydro-isoquinoline is reacted with sodium triacetoxyborohydride to provide the title compound.

출처 및 근거

ORD 기록: ord-824039881986465c9704711edebc5419
출처 데이터셋: uspto-grants-2011_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07985753B2

반응 노트

불러오는 중…