Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → HCID 10443568, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 2-Aminoheptane | HCID 5603 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | HCID 10443568 | HCID 10443568 | — |
반응 단계
100 ml of methanol and 100 mmol of 2-heptylamine are initially taken and 100 mmol of benzaldehyde are added dropwise at 24° C. in the course of 15 minutes. Stirring is effected for 6 hours at 24° C., the completeness of the iminization is checked by GC, 0.5 g of Pd/C (10% by weight) is added and the crude mixture is hydrogenated with hydrogen for 5 hours at atmospheric pressure. A sample is taken and the composition is investigated by GC analysis.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06476268B1 |
| 출처 데이터셋 | uspto-grants-2002_11 |
| ORD ID | ord-ba1edca4717347c4aa02c2f111f30d6f |
| 출처 메모 | uspto-grants-2002_11 |