Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 6-Methyl-5-nitroquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 6-Methylquinoline | HCID 7059 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | 6-Methyl-5-nitroquinoline | HCID 90009 | — |
반응 단계
2.45 mol of 6-methylquinoline were added to 1 l of concentrated sulfuric acid, and 2.94 mol of 65% strength nitric acid were added dropwise at from 0 to 10° C. The mixture was stirred for one hour, poured onto ice, adjusted to pH 2.5 using aqueous sodium hydroxide solution, filtered off with suction, washed with water and dried over magnesium sulfate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06479436B1 |
| 출처 데이터셋 | uspto-grants-2002_11 |
| ORD ID | ord-fba0f63ffa8d41a3a1766704edbaa66d |
| 출처 메모 | uspto-grants-2002_11 |