1,2-Ethanediamine, N1-phenyl- → 2-Chloro-6-[2-(phenylamino)ethylamino]-9-cyclopentylpurine

HRID 1017317

반응식

HRID 1017317 반응식
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4](Cl)[N:3]=1.[C:17]1([NH:23][CH2:24][CH2:25][NH2:26])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C(N(CC)CC)C>[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4]([NH:26][CH2:25][CH2:24][NH:23][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[N:3]=1

참가 물질

4

반응물 2

HCID 742701,2-Ethanediamine, N1-phenyl-HCID 108011162,6-dichloro-9-cyclopentyl-9H-purine

생성물 1

HCID 180022562-Chloro-6-[2-(phenylamino)ethylamino]-9-cyclopentylpurine

시약·촉매·용매 1

HCID 8471Triethylamine용매

실험 절차

2-Chloro-6-[2-(phenylamino)ethylamino]-9-cyclopentylpurine is prepared from 2,6-dichloro-9-cyclopentylpurine, N-phenylethylenediamine, and triethylamine essentially as described above in Example 1, Scheme A, step b.

출처 및 근거

ORD 기록
ord-67d155c980ef4e4c8d7ab6ba5bfd77be
출처 데이터셋
uspto-grants-2002_11
특허 번호
US06479487B1

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