Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aluminum(III) Chloride → 4-Iodo-3-nitro-benzophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 반응물 | 4-Iodo-3-nitrobenzoic acid | HCID 11208598 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 4-Iodo-3-nitro-benzophenone | HCID 11187302 | — |
반응 단계
5.3 g (17 mmol) of 4-iodo-3-nitrobenzoic acid and 8.0 g (60 mmol) of aluminium trichloride are added successively to 70 ml of benzene while cooling with an ice bath. Then the mixture is stirred for 2 hours at ambient temperature, then poured into ice water, extracted with methylene chloride, dried with sodium sulphate and concentrated in vacuo.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06479524B1 |
| 출처 데이터셋 | uspto-grants-2002_11 |
| ORD ID | ord-2af6b35e3597405292621887034b7779 |
| 출처 메모 | uspto-grants-2002_11 |