Thionyl Chloride → HCID 82633711, 화합물

HRID 1017798노트

반응식

HRID 1017798 반응식
[Br:1][C:2]1[C:10]([CH3:11])=[CH:9][C:5]([C:6](O)=[O:7])=[C:4]([CH3:12])[CH:3]=1.S(Cl)([Cl:15])=O>ClCCl>[Br:1][C:2]1[C:10]([CH3:11])=[CH:9][C:5]([C:6]([Cl:15])=[O:7])=[C:4]([CH3:12])[CH:3]=1

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 27534794-Bromo-2,5-dimethylbenzoic acid

생성물 1

HCID 82633711HCID 82633711, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

10.3 g (45 mmol) of 4-bromo-2,5-dimethylbenzoic acid are dissolved in 250 ml of dichloromethane and after the addition of 9.9 ml of (135 mmol) of thionyl chloride refluxed for two hours. Then the mixture is evaporated to dryness.

후처리

  1. temperaturerefluxed for two hours
  2. customThen the mixture is evaporated to dryness

출처 및 근거

ORD 기록
ord-18404acdd5ac40eea2a7fb1202460710
출처 데이터셋
uspto-grants-2002_11
특허 번호
US06479524B1

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