Hydrazine → HCID 178518899, 화합물

HRID 1018932

반응식

HRID 1018932 반응식
[NH2:1][NH2:2].[Cl:3][C:4]1[CH:20]=[CH:19][C:7]([C:8]([C:10]2[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=2[C:12](O)=[O:13])=O)=[CH:6][CH:5]=1>>[Cl:3][C:4]1[CH:20]=[CH:19][C:7]([C:8]2[C:10]3[C:11](=[CH:15][CH:16]=[CH:17][CH:18]=3)[C:12]([OH:13])=[N:2][N:1]=2)=[CH:6][CH:5]=1

참가 물질

3

반응물 2

HCID 9321HydrazineHCID 665642-(4'-Chlorobenzoyl)benzoic acid

생성물 1

HCID 178518899HCID 178518899, 화합물

실험 절차

A 3 M ethanolic solution of hydrazine (20 ml, 60 mmol) is added to 2-(4-chlorobenzoyl)benzoic acid (5.5 g, 20 mmol), and the mixture is stirred at room temperature for 5 hours. Precipitation gives 4-(4-chlorophenyl)-1-hydroxy-phthalazine.

후처리

  1. customPrecipitation

출처 및 근거

ORD 기록
ord-c77d4794478546fdb5436fdcb611d420
출처 데이터셋
uspto-grants-2002_11
특허 번호
US06486158B1

연결된 노트

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