Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4'-(2,4,5-Triphenylimidazol-1-yimethyl)biphenyl-2-sulfonic Acid Dimethylaminomethylenamide → 4'-(2,4,5-Triphenylimidazol-1-ylmethyl)biphenyl-2-sulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4'-(2,4,5-Triphenylimidazol-1-yimethyl)biphenyl-2-sulfonic Acid Dimethylaminomethylenamide | HCID 70144593 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4'-(2,4,5-Triphenylimidazol-1-ylmethyl)biphenyl-2-sulfonamide | HCID 18400113 | 58% |
반응 단계
1.9 g of 4′-(2,4,5-triphenylimidazol-1-ylmethyl)biphenyl-2-sulfonic acid dimethylaminomethylenamide in 20 ml of ethanol and 20 ml of a saturated aqueous HCl solution are refluxed for 3 h. The volatile constituents are removed in vacuo, the residue is stirred with 100 ml of water and the product is filtered off. 1.0 g of an amorphous powder is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06486189B2 |
| 출처 데이터셋 | uspto-grants-2002_11 |
| ORD ID | ord-2819804ff7e8469ab870846ac50f3c59 |
| 출처 메모 | uspto-grants-2002_11 |