Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methoxy-5-nitro-2-(pyrrolidin-1-yl)pyridine → 4-Methoxy-2-(pyrrolidin-1-yl)-5-aminopyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methoxy-5-nitro-2-(pyrrolidin-1-yl)pyridine | HCID 57431518 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | 4-Methoxy-2-(pyrrolidin-1-yl)-5-aminopyridine | HCID 57431519 | 96.3% |
반응 단계
The method described in Stage 12.2 is followed, starting from 1.5 g (6.72 mmol) of 4-methoxy-5-nitro-2-(pyrrolidin-1-yl)-pyridine, obtained in Stage 6.1, and 0.15 g of palladium on charcoal at 10%. We thus obtain 1.25 g of the expected product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08716273B2 |
| 출처 데이터셋 | uspto-grants-2014_05 |
| ORD ID | ord-2e71675bb5244e4896652bfab9997d2b |
| 출처 메모 | uspto-grants-2014_05 |