Phenylacetylene → (5-Phenylethynyl-pyridin-2-yl)-methanol

HRID 1020183노트

반응식

Br[C:2]1[CH:3]=[CH:4][C:5]([CH2:8][OH:9])=[N:6][CH:7]=1.[C:10]1([C:16]#[CH:17])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[C:10]1([C:16]#[C:17][C:2]2[CH:3]=[CH:4][C:5]([CH2:8][OH:9])=[N:6][CH:7]=2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

참가 물질

반응물 2

HCID 10821Phenylacetylene

HCID 5200169(5-Bromopyridin-2-yl)methanol

생성물 1

HCID 57517077(5-Phenylethynyl-pyridin-2-yl)-methanol

실험 절차

The title compound, light brown solid, MS: m/e=210.2 (M+H+), can be prepared in accordance with the general method of example 1, step 1 from (5-bromopyridin-2-yl)methanol and phenylacetylene.

출처 및 근거

ORD 기록: ord-fd7cd4b8b5df4d25982fabd54a4b19ee
출처 데이터셋: uspto-grants-2014_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08716316B2

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