Phenylacetylene → rac-1-(5-Phenylethynyl-pyridin-2-yl)-ethanol

HRID 1020195노트

반응식

HRID 1020195 반응식
Br[C:2]1[CH:3]=[CH:4][C:5]([CH:8]([OH:10])[CH3:9])=[N:6][CH:7]=1.[C:11]1([C:17]#[CH:18])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:11]1([C:17]#[C:18][C:2]2[CH:3]=[CH:4][C:5]([CH:8]([OH:10])[CH3:9])=[N:6][CH:7]=2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

참가 물질

3

반응물 2

HCID 10821PhenylacetyleneHCID 426142881-(5-Bromopyridin-2-yl)ethanol

생성물 1

HCID 57517078rac-1-(5-Phenylethynyl-pyridin-2-yl)-ethanol

실험 절차

The title compound, brown solid, MS: m/e=224.2 (M+H+), can be prepared in accordance with the general method of example 31, step 1 from rac-1-(5-bromopyridin-2-yl)ethanol and phenylacetylene.

출처 및 근거

ORD 기록
ord-a125d9d73c9b4be49cfa8b90d0a5d362
출처 데이터셋
uspto-grants-2014_05
특허 번호
US08716316B2

반응 노트

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