4-Phenylpiperidine → HCID 57461791, 화합물

반응식

Cl[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-])=O)=[CH:4][N:3]=1.[C:11]1([CH:17]2[CH2:22][CH2:21][NH:20][CH2:19][CH2:18]2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:11]1([CH:17]2[CH2:18][CH2:19][N:20]([C:2]3[N:3]=[CH:4][C:5]([NH2:8])=[CH:6][CH:7]=3)[CH2:21][CH2:22]2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

참가 물질

반응물 2

HCID 698734-Phenylpiperidine

HCID 783082-Chloro-5-nitropyridine

생성물 1

HCID 57461791HCID 57461791, 화합물

실험 절차

Intermediate B-6 was prepared by the general procedure for intermediate B-2, by using 2-chloro-5-nitropyridine and 4-phenylpiperidine as starting materials. LCMS (ESI) calcd for [M+1]+ 254.2. found 254.1.

후처리

customIntermediate B-6 was prepared by the general procedure for intermediate B-2

출처 및 근거

ORD 기록: ord-f8d3d404e765422d9c1fb64d85a7d903
출처 데이터셋: uspto-grants-2014_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08716312B2

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